苯并[b]荧蒽检测

T/ZFB 0008-2020 纺织品 苯并(b)荧蒽的测定 高效液相色谱法

4　原理 用甲醇超声提取纺织产品中的苯并(b)荧蒽物质，提取液经滤膜过滤后，采用高效液相色谱仪-荧光检测器(HPLC-FLD)测定和确证，外标法定量。 5　试剂和材料 5.1　试剂 5.1.1　甲醇：色谱纯。 5.1.2　水：GB/T 6682规定的二级水。 5.2　标准品 苯并(b)荧蒽标准品：纯度≥99%，化合物信息见附录A。 5.3　标准溶液配置 5.3.1　标准储备溶液（100 mg/L）：准确称取适量苯并(b)荧蒽标准品（5.2），用甲醇（5.1.1）配制成浓度为100.0 mg/L的储备溶液。 注：标准储备溶液保存在棕色瓶中，存储于0℃-4℃冰箱中，有效期3个月。 5.3.2　标准中间液（1000 μg/L）：准确移取标准储备溶液（100 mg/L）1.00 mL于100 mL容量瓶中，加甲醇至刻度，混匀。 注：标准工作溶液存储于0 ℃-4 ℃冰箱中。 5.3.3　标准工作溶液：分别移取标准中间液（1000 μg/L）0.20 mL、0.50 mL、1.00 mL、5.00 mL和10.00 mL于100 mL容量瓶中，加甲醇至刻度，混匀。此系列标准工作溶液质量浓度分别为2.00 μg/L、5.00 μg/L、10.00 μg/L、50.00 μg/L和100 μg/L。 注：标准工作溶液存储于0 ℃-4 ℃冰箱中。 6　仪器和设备 6.1　反应器：具塞玻璃比色管，约50 mL。 6.2　高效液相色谱仪：配有荧光检测器（FLD）。 6.3　超声波发生器：超声功率不低于270 W，超声频率50 kHz～60 kHz，温度控制范围25℃～60℃。 6.4　有机相针式过滤头（聚四氟乙烯）：孔径0.45 μm。 6.5　容量瓶：100 mL。 6.6　电子天平：分度值为0.1 mg。 6.7　移液管：1 mL、5 mL、10 mL.

Textiles—Determination of benzo[b]fluoranthene—High performance liquid chromatography

ASTM D7881-20e1 用反向电压模式的毛细管电泳测定纯化对苯二甲酸中4-羧基苯甲醛和

Standard Test Method for Determination of 4-Carboxybenzaldehyde and p-Toluic Acid in Purified Terephthalic Acid by Capillary Electrophoresis with Reverse Voltage Mode

ASTM D7881-20 用反向电压模式的毛细管电泳测定纯化对苯二甲酸中4-羧基苯甲醛和

Standard Test Method for Determination of 4-Carboxybenzaldehyde and p-Toluic Acid in Purified Terephthalic Acid by Capillary Electrophoresis with Reverse Voltage Mode

ASTM D7883-20 通过弱阴离子交换高效液相色谱法测定纯化对苯二甲酸中的4-羧基苯甲醛和

Standard Test Method for Determination of 4-Carboxybenzaldehyde and p-Toluic Acid in Purified Terephthalic Acid by Weak Anion Exchange High Performance Liquid Chromatography

ASTM D7881-19 用反向电压模式的毛细管电泳测定纯化对苯二甲酸中4-羧基苯甲醛和

Standard Test Method for Determination of 4-Carboxybenzaldehyde and p-Toluic Acid in Purified Terephthalic Acid by Capillary Electrophoresis with Reverse Voltage Mode

ASTM D7883-19 通过弱阴离子交换高效液相色谱法测定纯化对苯二甲酸中的4-羧基苯甲醛和

Standard Test Method for Determination of 4-Carboxybenzaldehyde and p-Toluic Acid in Purified Terephthalic Acid by Weak Anion Exchange High Performance Liquid Chromatography

NF V03-169-2015 食品分析. 使用气相色谱-质谱法 (GC-MS) 测定食品中的苯并(a)芘, 苯并(a)蒽, 稠二萘以及苯并(b)荧蒽

Food analysis - Determination of benzo(a)pyrene, benz(a)anthracene, chrysene and benzo(b)fluoranthene in foodstuffs by gas chromatography mass spectrometry (GC-MS)

BS EN 16619-2015 食品分析. 采用气相色谱质谱 (GC-MS) 联用技术对食品中苯并[a]芘, 苯并[a]蒽, 屈以及苯并[b]荧蒽的测定

Food analysis. Determination of benzo[a]pyrene, benz[a]anthracene, chrysene and benzo[b]fluoranthene in foodstuffs by gas chromatography mass spectrometry (GC-MS)

BS PD CEN/TS 16621-2014 食品分析. 采用带荧光检测的高效液相色谱法(HPLC-FD)对食品中苯并[a]芘, 苯并[a]蒽, 屈以及苯并[b]荧蒽的测定

Food analysis. Determination of benzo[a]pyrene, benz[a]anthracene, chrysene and benzo[b]fluoranthene in foodstuffs by high performance liquid chromatography with fluorescence detection (HPLC-FD)

BS PD CEN/TS 16645-2014 环境空气. 苯并[a]蒽, 苯并[b]荧蒽, 苯并[j]荧蒽, 苯并[k]荧蒽, 二苯并[a,h]蒽, 茚并[1,2,3-cd]芘以及苯并[ghi]苝的测量方法

Ambient air. Method for the measurement of benz[a]anthracene, benzo[b]fluoranthene, benzo[j]fluoranthene, benzo[k]fluoranthene, dibenz[a,h]anthracene, indeno[1,2,3-cd]pyrene and benzo[ghi]perylene

PD CEN/TS 16645-2014 环境空气.苯并[a]蒽,苯并[b]荧蒽,苯并[ J ]荧蒽,苯并[K]荧蒽,二苯并[a，h]蒽，茚并[1,2,3-cd]芘和苯并[ghi]苝的测量方法

This Technical Specification specifies a measurement method for the determination of the particle bound polycyclic aromatic hydrocarbon (PAH) compounds benz[a]anthracene (BaA), benzo[b]fluoranthene (BbF), benzo[j]fluoranthene (BjF), benzo[k]fluoranthene (BkF), dibenz[a,h]anthracene (DBahA), indeno[1,2,3-cd]pyrene (INP) and benzo[ghi]perylene (BghiP) in ambient air, which can be used in the framework of Council Directive 2008/50/EC and Directive 2004/107/EC. This document specifies performance characteristics and performance criteria for this measurement method. The performance characteristics of the measurement method are based on a sampling period of 24 h. This Technical Specification describes a measurement method which comprises sampling of the selected PAH compounds as part of the PM10 particles, sample extraction and analysis by high performance liquid chromatography (HPLC) with fluorescence detector (FLD) or by gas chromatography with mass spectrometric detection (GC-MS). The method is applicable for the measurement of the PAH compounds in the concentration range from approx. 0,04 ng/m 3 to approximately 20 ng/m 3 for BaA, BbF, BjF, BkF, BaP, INP and BghiP and 0,02 ng/m 3 to approximately 2 ng/m 3 for DBahA. Table 1 shows examples for concentrations of the compounds (annual mean values) for sampling sites with different characteristics. The lower limit of the applicable range depends on the noise level of the detector and the variability of the laboratory filter blank.

Ambient air - Method for the measurement of benz[a]anthracene@ benzo[b]fluoranthene@ benzo[j]fluoranthene@ benzo[k]fluoranthene@ dibenz[a@h]anthracene@ indeno[1@2@3- cd]pyrene and benzo[ghi]perylene

PD CEN/TS 16621-2014 食品分析.用高效液相色谱荧光检测法（HPLC-FD）检测食品中的苯并[a]芘,奔驰[a]蒽,屈和苯并[b]荧蒽

This Technical Specification specifies a method for the determination of benzo[a]pyrene (BaP) plus benz[a]anthracene (BaA), benzo[b]fluoranthene (BbF) and chrysene (CHR) in several food matrices. The method is based on size exclusion chromatography (SEC) cleanup, followed by quantification with high performance liquid chromatography (HPLC) with programmable fluorescence detection. This method has been in-house validated via the analysis of spiked samples of edible olive oil, fresh mussels, smoked fish, smoked meat products, processed cereal-based foods for young children, infant formulae, chocolate and food supplements (isoflavones) at levels ranging from 0,25 g/kg to 1,00 g/kg and from 4,95 g/kg to 23,53 µg/kg, depending on the Polycyclic Aromatic Hydrocarbon (PAH) or the matrix. This method complies with the performance characteristics specified for BaP, BaA, BbF and CHR in current legislation. The method has been shown to be applicable to a variety of additional matrices as meat products, fresh fish, paprika, roasted coffee, bread, herbs, breakfast cereals, beer, sunflower oil, olives and fried tomato, with a limit of quantification below 0,5 µg/kg. In addition, the method was tested in-house and shown to be applicable also for the quantification of the other 12 PAHs of the 15+1 EU priority PAHs set (benzo[c]fluorene (BcL), benzo[j]fluoranthene (BjF), benzo[k]fluoranthene (BkF), cyclopenta[cd]pyrene (CPP), dibenz[a,h]anthracene (DhA), dibenzo[a,e]pyrene (DeP), benzo[ghi]perylene (BgP), dibenzo[a,h]pyrene (DhP), dibenzo[a,i]pyrene (DiP), dibenzo[a,l]pyrene (DlP), indeno[1,2,3-cd]pyrene (IcP), 5-methylchrysene (5MC)) in all matrices listed above and at similar level ranges, except for CPP, where a UV detection had to be used with limits of quantification above 8 µg/kg. For the determination of PAHs in edible fats and oils, two other standards are also available, EN ISO 22959 and EN ISO 15753.

Food analysis - Determination of benzo[a]pyrene@ benz[a]anthracene@ chrysene and benzo[b]fluoranthene in foodstuffs by high performance liquid chromatography with fluorescence detection (HPLC-FD)

CFR 21-520.38b-2013 食品和药物. 第520部分:新型口服动物药剂. 第520.38b节:阿苯达唑膏.

(a) Specifications. The product contains 30 percent albendazole. (b) Sponsor. See No. 000069 in § 510.600(c) of this chapter. (c) Related tolerances. See § 556.34 of this chapter. (d) Conditions of use in cattle(1) Amount. Equivalent to 4.54 milligrams p

Food and drugs. Part520:Oral dosage form new animal drugs. Section520.38b:Albendazole paste.

ASTM D7881-13 用反向电压模式的毛细管电泳测定纯化对苯二甲酸中4-羧基苯甲醛和

Standard Test Method for Determination of 4-Carboxybenzaldehyde and p-Toluic Acid in Purified Terephthalic Acid by Capillary Electrophoresis with Reverse Voltage Mode

ASTM D7883-13 通过弱阴离子交换高效液相色谱法测定纯化对苯二甲酸中的4-羧基苯甲醛和

Standard Test Method for Determination of 4-Carboxybenzaldehyde and p-Toluic Acid in Purified Terephthalic Acid by Weak Anion Exchange High Performance Liquid Chromatography

DIN EN 15980-2011 空气质量.苯并(a)蒽,苯并(b)荧蒽,苯并(j)荧蒽,苯并(k)荧蒽,苯并[a]芘,二苯并(a,h)蒽和茚并[1,2,3-cd]芘沉积物的测定,德文版本EN 15980-2011

This document specifies a method for the determination of the atmospheric deposition of benz[a]anthracene (BaA), benzo[b]fluoranthene (BbF), benzo[j]fluoranthene (BjF), benzo[k]fluoranthene (BkF), benzo[a]pyrene (BaP), dibenz[a,h]anthracene (DBahA) and indeno[1,2,3-cd]pyrene (INP), that can, for example, be used in the framework of Council Directive 2004/107/EC. The Standard specifies performance requirements with which the methods have to comply in order to meet the data quality objectives given in this Directive. This document specifies methods for sampling, sample preparation and analysis using gas chromatography with mass spectroscopic detection (GC/MS) or high performance liquid chromatography with fluorescence detection (HPLC/FLD)). The funnel-bottle bulk collector is used as the standard collector.

Air quality - Determination of the deposition of benz[a]anthracene, benzo[b]fluoranthene, benzo[j]fluoranthene, benzo[k]fluoranthene, benzo[a]pyrene, dibenz[a,h]anthracene and indeno[1,2,3-cd]pyrene; German version EN 15980:2011

NF X43-357-2011 空气质量.测定沉积的苯(a)蒽,苯并(b)荧蒽,苯并(j)荧蒽,苯并(k)荧蒽,苯并(a)芘,二苯蒽(a,h)和茚并(1,2,3-cd)芘.

Air quality - Determination of the deposition of benz(a)anthracene, benzo(b)fluoranthene, benzo(j)fluoranthene, benzo(k)fluoranthene, benzo(a)pyrene, dibenz(a,h)anthracene and indeno(1,2,3-cd)pyrene.

BS EN 15980-2011 空气质量.苯[a]蒽,苯并[b]荧蒽,苯并[j]荧蒽,苯并[k]荧蒽,苯并[a]芘,二苯[a,h]蒽和茚并[1,2,3-cd]芘沉积物的测定

This document specifies a method for the determination of the bulk deposition of benz[a]anthracene (BaA), benzo[b]fluoranthene (BbF), benzo[j]fluoranthene (BjF), benzo[k]fluoranthene (BkF), benzo[a]pyrene (BaP), dibenz[a,h]anthracene (DBahA) and indeno[1,2,3-cd]pyrene (INP), which can be used in the framework of Directive 2004/107/EC. This European Standard specifies performance requirements with which the method has to comply in order to meet the data quality objectives given in this Directive. This document specifies methods for sampling, sample preparation and analysis using gas chromatography with mass spectroscopic detection (GC/MS) or high performance liquid chromatography with fluorescence detection (HPLC/FLD). The funnel-bottle bulk collector is used as the standard collector. The method is applicable for deposition measurements in  rural and remote areas,  industrial areas,  urban areas. The standard is applicable in the range from a few ng/(m⋅ d) to a few hundred ng/(m⋅ d).

Air quality. Determination of the deposition of benz[a]anthracene, benzo[b]fluoranthene, benzo[j]fluoranthene, benzo[k]fluoranthene, benzo[a]pyrene, dibenz[a,h]anthracene and indeno[1,2,3-cd]pyrene

EN 15980-2011 空气质量.测定苯并[a]蒽,苯并[b]荧蒽,苯并[J]荧蒽,苯并[k]荧蒽,苯并[a]芘,二苯并[A,H]蒽和茚并[1的沉积,2,3-CD]芘

This document specifies a method for the determination of the bulk deposition of benz[a]anthracene (BaA), benzo[b]fluoranthene (BbF), benzo[j]fluoranthene (BjF), benzo[k]fluoranthene (BkF), benzo[a]pyrene (BaP), dibenz[a,h]anthracene (DBahA) and indeno[1,2,3-cd]pyrene (INP), which can be used in the framework of Directive 2004/107/EC.This European Standard specifies performance requirements with which the method has to comply in order to meet the data quality objectives given inThis Directive.This document specifies methods for sampling, sample preparation and analysis using gas chromatography with mass spectroscopic detection (GC/MS) or high performance liquid chromatography with fluorescence detection (HPLC/FLD). The funnel-bottle bulk collector is used as the standard collector. The method is applicable for deposition measurements in:-rural and remote areas,- industrial areas;- urban areas. The standard is applicable in the range from a few ng/(m2 · d) to a few hundred ng/(m2 · d).

Air quality - Determination of the deposition of benz[a]anthracene, benzo[b]fluoranthene, benzo[j]fluoranthene, benzo[k]fluoranthene, benzo[a]pyrene, dibenz[a,h]anthracene and indeno[1,2,3-cd]pyrene

FORD ESF-M4D405-D-2010 聚乙烯对苯二甲酸酯(PET),35%玻璃纤维/云母增强模塑材料***与福特WSS-M99P1111-A***一起使用.在福特ESF-M4D405-B中显示

POLYETHYLENE TEREPHTHALATE (PET), 35 % GLASS FIBER/MICA REINFORCED MOLDING COMPOUND ***TO BE USED WITH FORD WSS-M99P1111-A*** (Shown on FORD ESF-M4D405-B)

FORD ESF-M4D405-D2-2010 聚乙烯对苯二甲酸酯(PET),45%玻璃纤维/矿物增强模塑材料***与福特WSS-M99P1111-A***一起使用.在福特ESF-M4D405-B中显示

POLYETHYLENE TEREPHTHALATE (PET), 45 % GLASS FIBER/MINERAL REINFORCED MOLDING COMPOUND ***TO BE USED WITH FORD WSS-M99P1111-A***

M 361-2004 责成欧洲标准化委员会对苯并芘及其他聚合芳香烃如苯并(a)蒽,苯并(b)荧蒽,苯并(j)荧蒽,苯并(k)荧蒽,茚并(1,2,3-c,d)蒽和二苯(a,h)蒽的沉积物总量的标准测量方法进行标准化的委托书

STANDARDISATION MANDATE TO CEN FOR STANDARD MEASURING METHODS FOR THE DETERMINATION OF TOTAL DEPOSITION OF BENZO(A)PYRENE AND OTHER POLYCYLIC AROMATIC HYDROCARBONS SUCH AS BENZO(A)ANTHRACENE, BENZO(B)FLUORANTHENE, BENZO(J)FLUORANTHENE, BENZO(K)FLUORANTHEN

FORD ESF-M4D405-D2-1992 45%玻璃纤维/矿物材料增强的聚对苯二甲酸乙二酯（PET）．列于标准ESF-M4D405-B上

POLYETHYLENE TEREPHTHALATE (PET), 45 % GLASS FIBER/MINERAL REINFORCED MOLDING COMPOUND Shown on ESF-M4D405-B

FORD ESF-M4D405-D-1992 35%玻璃纤维/云母增强的聚对苯二甲酸乙二酯（PET）．列于标准ESF-M4D405-B上

POLYETHYLENE TEREPHTHALATE (PET), 35 % GLASS FIBER/MICA REINFORCED MOLDING COMPOUND Shown on ESF-M4D405-B

PN C04544-01-1987 水和废水.多环芳香烃的含量试验. 使用二维薄层色谱法测定水中苯并[a]芘、苯并[b]荧蒽、苯并[k]荧蒽、苯并[ ghi]二萘嵌苯、荧蒽和茚并( 1,2,3-cd)芘的含量

Water and waste water -- Tests for content of polycyclic aromatic hydrocarbons (PAH) -- Determination of benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, benzo(ghi)perylene, fluoranthene and indeno (1,2,3-c,d)pyrene in water by two-dimensional