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本标准规定了饲料中玉米赤霉烯酮含量的免疫亲和柱净化高效液相色谱的测定方法。 本标准适用于饲料中玉米赤霉烯酮的测定。 本标准的检测限为2μg/kg,定量限为10μg/kg.
Determination of zearalenone in feed.High performance liquid chromatographic method with immunoaffinity column clean-up
本标准规定了食品中玉米赤霉烯酮含量的免疫亲和层析净化高效液相色谱测定方法。 本标准适用于粮食和粮食制品、酒类、酱油、醋、酱及酱制品中玉米赤霉烯酮含量的测定。 本标准的方法检出限：粮食和粮食制品的检出限为20 μg/kg，酒类的检出限为20 μg/kg，酱油、醋、酱及酱制品的检出限为50 μg/kg。
Determination of zearalenone in food.High performance liquid chromatographic method with immunoaffinity column clean-up
本标准规定了谷物中玉米赤霉烯酮的测定方法。 本标准适用于谷物（玉米、小麦等）中玉米赤霉烯酮的测定。 本标准方法检出限为5μg/kg。
Determination of zearalenone in cereals
本标准规定了动物源食品中玉米赤霉醇、β-玉米赤霉醇、α-玉米赤霉烯醇、β-玉米赤霉烯醇、玉米赤霉酮和玉米赤霉烯酮残留量的液相色谱-质谱/质谱测定方法。 本标准适用于牛肉、猪肉、牛肝、牛奶和鸡蛋中玉米赤霉醇、β-玉米赤霉醇、α-玉米赤霉烯醇、β-玉米赤霉烯醇、玉米赤霉酮和玉米赤霉烯酮残留量的定性确证和定量测定。
Determination of residues of zearalanol,β-zearalanol,α-zearalenol,β-zearalenol,zearalanone and zearalenone in foodstuffs of animal origin.LC-MS/MS method
本标准规定了饲料中玉米赤霉烯酮(ZEN)和赭曲霉毒素A(OA)的允许量。 本标准适用于配合饲料和玉米。
Hygienical standard for feeds.Toleration of ochratoxin A and zearalenone in feeds
本标准规定了玉米赤霉烯酮(zearalenone，以下简称ZEN)的薄层色谱测定方法和酶联免疫吸附测定法。 本标准适用于配合饲料和饲用谷物原料中ZEN的测定。 薄层色谱测定方法的最低检测量为20 n9，酶联免疫吸附测定方法的最低检测量为0．25 n9。
Determination of zearalenone in feeds
因地方标准信息公布不透明，地方标准有效性更新或有延迟，望大家理解。
原理将样品提取物滴入检测卡加样处，提取物中的霉菌毒素在反应区（T线）竞争性地与霉 菌毒素单克隆抗体-UCP反应，在反应区（T线）形成固相抗原-标记抗体-UCP（Up-Converting Phosphor，上转发光材料）颗粒复合物。反应区（T线）和质控区（C线）UCP颗粒在激发光 下发出可见光信号，上转发光免疫分析仪获得反应区对应的T值与质控区对应的C值。T/C比 值与试样中的黄曲霉毒素B1、玉米赤霉烯酮和呕吐毒素含量成反比。
Rapid determination of aflatoxin B1, zearalenone, and deoxynivalenol in feeds - upconversion luminescence (UPT) method
因地方标准信息公布不透明，地方标准有效性更新或有延迟，望大家理解。本文件规定了玉米赤霉烯酮降解酶（zearalenone-degradingenzyme，英文缩写：ZHD）的活力检测方法。本文件适用于玉米赤霉烯酮降解酶产品，最低检出量为0.2U/g（U/mL）。
将定量的非金属矿物材料与一定浓度的玉米赤霉烯酮溶液作用，通过测试达到平衡后上清液中玉米赤霉烯酮含量变化计算吸附率，用吸附率评价非金属矿物材料的脱霉性能。 将吸附实验后离心沉淀物与定量的不含玉米赤霉烯酮溶液作用，通过测试达到平衡后上清液内玉米赤霉烯酮含量变化计算解吸率，用解吸率评价非金属矿物材料脱霉性能的稳定性。
Test Method for Removal of Zearalenone by Nonmetallic Mineral Materials
本标准规定了饲草中脱氧雪腐镰刀菌烯醇和玉米赤霉烯酮的液相色谱-串联质谱测定方法。本标准适用于饲草中脱氧雪腐镰刀菌烯醇和玉米赤霉烯酮的测定。本方法检出限：脱氧雪腐镰刀菌烯醇为10 μg/kg和玉米赤霉烯酮为5 μg/kg；定量限：脱氧雪腐镰刀菌烯醇为25 μg/kg和玉米赤霉烯酮为10 μg/kg。
本标准规定了饲草中脱氧雪腐镰刀菌烯醇和玉米赤霉烯酮的液相色谱-串联质谱测定方法。 本标准适用于饲草中脱氧雪腐镰刀菌烯醇和玉米赤霉烯酮的测定。 本方法检出限：脱氧雪腐镰刀菌烯醇为10 μg/kg和玉米赤霉烯酮为5 μg/kg；定量限：脱氧雪腐镰刀菌烯醇为25 μg/kg和玉米赤霉烯酮为10 μg/kg。 已废止 公告：山东省市场监管局关于废止畜牧兽医领域360项山东省地方标准（计划）的公告 2021年第6号
本标准规定了饲料中黄曲霉毒素B1、呕吐毒素、伏马毒素B1和玉米赤霉烯酮含量测定的高效液相色谱—串联质谱测定方法。 本标准适用于饲料原料、配合饲料、浓缩饲料、精料补充料、添加剂预混料中黄曲霉毒素B1、呕吐毒素、伏马毒素B1和玉米赤霉烯酮含量的测定。 本方法中黄曲霉毒素B1、呕吐毒素、伏马毒素B1和玉米赤霉烯酮的检出限为0.005 μg/kg、10 μg/kg、10 μg/kg和0.10 μg/kg。 已废止 公告：山东省市场监管局关于废止畜牧兽医领域360项山东省地方标准（计划）的公告 2021年第6号
本标准规定了饲料中黄曲霉毒素B1、呕吐毒素、伏马毒素B1和玉米赤霉烯酮含量测定的高效液相色谱—串联质谱测定方法。本标准适用于饲料原料、配合饲料、浓缩饲料、精料补充料、添加剂预混料中黄曲霉毒素B1、呕吐毒素、伏马毒素B1和玉米赤霉烯酮含量的测定。本方法中黄曲霉毒素B1、呕吐毒素、伏马毒素B1和玉米赤霉烯酮的检出限为0.005μg/kg、10μg/kg、10μg/kg和0.10μg/kg。
本标准规定了食品中玉米赤霉烯酮快速检测胶体金免疫层析法。本标准适用玉米、小麦及其碾磨加工品中玉米赤霉烯酮快速筛选测定。
因地方标准信息公布不透明，地方标准有效性更新或有延迟，望大家理解。本标准规定了饲料中玉米赤霉烯酮的胶体金快速定量检测方法的原理、试剂和材料、仪器设备、样品制备与留存、检测步骤和重复性。本标准适用于饲料产品及饲料原料中玉米赤霉烯酮的快速定量检测。检测限为50μg/kg，检测范围为50ug/kg～1000μg/kg。
本标准规定了小麦生产、收获、运输、储藏与加工过程中玉米赤霉烯酮类毒素污染控制的技术及要求。本标准适用于小麦生产、收获、运输、储藏与加工过程中玉米赤霉烯酮类毒素污染控制。
This method of analysis is applicable to the determination of HT-2 toxin (HT2) in the tested range of 22 µg/kg to 178 µg/kg, T-2 toxin (T2) in the tested range of 7 µg/kg to 50 µg/kg, Deoxynivalenol (DON) in the tested range of 88 µg/kg to 559 µg/kg, and Zearalenone (ZON) in the tested range of 14 µg/kg to 430 µg/kg in cereals and cereal-based compound animal feed. The actual working ranges may extend beyond the tested ranges. It is the responsibility of the laboratory to prove that the limit of quantitation (LOQ) for HT-2 and T-2 toxin is 10 µg/kg, for DON 100 µg/kg, and for ZON 20µg/kg.
Animal feeding stuffs: Methods of sampling and analysis - Determination of T-2 and HT-2 toxins@ Deoxynivalenol and Zearalenone@ in feed materials and compound feed by LCMS
Animal feeding stuffs. Determination of zearalenone by immunoaffinity column chromatography and high performance liquid chromatography
Animal feeding stuffs. Determination of zearalenone by immunoaffinity column chromatography and high performance liquid chromatography
本标准规定了饲料和饲料原料中黄曲霉毒素B1、黄曲霉毒素B2、黄曲霉毒素G1、黄曲霉毒素G2、玉米赤霉烯酮、脱氧雪腐镰刀菌烯醇、赭曲霉毒素A和T-2毒素的液相色谱-串联质谱测定方法。 本标准适用于植物性性饲料原料、配合饲料和浓缩饲料中黄曲霉毒素B1、黄曲霉毒素B2、黄曲霉毒素G1、黄曲霉毒素G2、玉米赤霉烯酮、脱氧雪腐镰刀菌烯醇、赭曲霉毒素A和T-2毒素含量的测定。
本标准规定了玉米赤霉烯酮的胶体金快速定量检测方法的原理、试剂、材料、仪器设备、样品制备、样品测定与结果表述。本标准适用于小麦、玉米和大米等粮食及其制品中玉米赤霉烯酮的快速定量检测。方法检测限为5 μg/kg。
Inspection of grain and oils.Detection of zearalenone in grain.Rapid quantitative method of colloidal gold technique
本标准规定了玉米赤霉烯酮的胶体金快速测试卡检测方法的原理、试剂及材料、仪器及设备、样品制备、样品测定、结果判定、阳性样品确认。本标准适用于小麦和玉米等谷物中玉米赤霉烯酮的快速筛查。
Inspection of grain and oils.Detection of zearalenone in cereal.Rapid method of colloidal gold technique
本标准规定了植物源性食品中α-玉米赤霉烯醇和赤霉烯酮液相色谱-质谱/质谱的测定方法。本标准适用于玉米、大豆、大米、花生、玉米淀粉、面粉、大豆油、玉米色拉油、芝麻油等植物源性食品中α-玉米赤霉烯醇和玉米赤霉烯酮的定性确证和定量测定。本标准方法检出限：α-玉米赤霉烯醇和玉米赤霉烯酮分别为1.5μg/kg和1.0μg/kg。
Animal feeding stuffs - Determination of zearalenone by immunoaffinity column chromatography and high performance liquid chromatography - Amendment 1 : limitation of the scope
Animal feeding stuffs - Determination of zearalenone by immunoaffinity column chromatography and high performance liquid chromatography - Amendment 1: Limitation of the scope
本标准规定了饲料中黄曲霉毒素、玉米赤霉烯酮和T-2毒素含量的液相色谱-串联质谱测定方法。 本标准适用于单一饲料、配合饲料、浓缩饲料、添加剂预混合饲料中黄曲霉毒素B1、黄曲霉毒素B2、黄曲霉毒素G1、黄曲霉毒素G2、玉米赤霉烯酮和T-2毒素含量的测定。 本标准各黄曲霉毒素与T-2毒素的检测限为1.0μg/kg,定量限为2.0μg/kg;玉米赤霉烯酮的检测限为5.0μg/kg,定量限为10.0μg/kg。
Determination of aflatoxias,zearaknone and T-2 in feeds. Liquid chromatography-tandem mass spectrometry
This European Standard specifies a method for the determination of zearalenone in maize based baby food, barley flour, maize flour, polenta, wheat flour and cereal based foods for infants and young children by high performance liquid chromatography (HPLC) with immunoaffinity cleanup and fluorescence detection. This method has been validated in two interlaboratory studies. The first study was for the analysis of samples of maize based baby food, barley flour, maize flour, polenta and wheat flour ranging from 10 μg/kg to 335 μg/kg, and the second study was for samples of cereal based foods for infants and young children ranging from 9 μg/kg to 44 μg/kg. Further information on validation, see Clause 9 and Annex B.
Foodstuffs - Determination of zearalenone in maize based baby food, barley flour, maize flour, polenta, wheat flour and cereal based foods for infants and young children - HPLC method with immunoaffinity column cleanup and fluorescence detection
This European Standard specifies a method for the determination of zearalenone in maize based baby food, barley flour, maize flour, polenta, wheat flour and cereal based foods for infants and young children by high performance liquid chromatography (HPLC) with immunoaffinity cleanup and fluorescence detection.This method has been validated in two interlaboratory studies. The first study was for the analysis of samples of maize based baby food, barley flour, maize flour, polenta and wheat flour ranging from 10 μg/kg to 335 μg/kg, and the second study was for samples of cereal based foods for infants and young children ranging from 9 μg/kg to 44 μg/kg. Further information on validation, see Clause 9 and Annex B.
Foodstuffs - Determination of zearalenone in maize based baby food, barley flour, maize flour, polenta, wheat flour and cereal based foods for infants and young children - HPLC method with immunoaffinity column cleanup and fluorescence detection
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