壬基苯酚检测

GB/T 29675-2013 化妆品中壬基苯酚的测定 液相色谱-质谱/质谱法

本标准规定了化妆品中壬基苯酚的液相色谱-质谱/质谱测定方法。本标准适用于膏霜、散粉、水剂、唇膏类化妆品中壬基苯酚的测定。本标准对于壬基苯酚的检出限为0.1 mg/kg,定量限为0.2 mg/kg。

Determination of nonylphenol in cosmetics.Liquid chromatography tandem mass spectrometry

T/CSIQ 78008-2020 食品塑料包装材料中壬基苯酚的测定 液相色谱-串联质谱法

本标准规定了液相色谱-串联质谱法测定食品塑料包装材料中壬基苯酚的方法。

Determination of nonyl phenol in food packaging plastic materials— Liquid chromatography-mass chromatography method

ASTM D7485-2016 采用液相色谱法/串联质谱法测定环境水体中壬基酚, 对叔辛基酚, 壬基酚乙和壬基苯酚二乙氧基醇的标准试验方法

5.1x00a0;NP and OP have been shown to have toxic effects in aquatic organisms. The source of NP and OP is prominently from the use of common commercial surfactants. The most widely used surfactant is nonylphenol ethoxylate (NPEO) which has an average ethoxylate chain length of nine. The ethoxylate chain is readily biodegraded to form NP1EO, NP2EO, nonylphenol carboxylate (NPEC) and, under anaerobic conditions, NP. NP will also biodegrade, but may be released into environmental waters directly at trace levels. This method has been investigated and is applicable for environmental waters, including seawater. 1.1x00a0;This test method covers the determination of nonylphenol (NP), nonylphenol ethoxylate (NP1EO), nonylphenol diethoxylate (NP2EO), and octylphenol (OP), extracted from water utilizing solid phase extraction (SPE), separated using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These compounds are qualitatively and quantitatively determined by this method. This method adheres to single reaction monitoring (SRM) mass spectrometry. 1.2x00a0;The method detection limit (MDL) and reporting limit (RL) for NP, NP1EO, NP2EO, and OP are listed in Table 1. (A)x00a0;MDL Determined Following The Code of Federal Regulations, 40 CFR Part 136, Appendix B.(B)x00a0;Lowest Point of the Reporting Range is Calculated from the LV 1 Concentration Calibration Standard in Table 4. 1.3x00a0;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4x00a0;This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Determination of Nonylphenol, p-tert-Octylphenol, Nonylphenol Monoethoxylate and Nonylphenol Diethoxylate in Environmental Waters by Liquid Chromatography/Tandem Mass Spectrometry

SN/T 4146-2015 化妆品中壬基苯酚的测定 液相色谱-质谱/质谱法

本标准规定了化妆品中壬基苯酚的液相色谱-质谱/质谱测定方法。 本标准适用于膏霜、散粉、水剂、唇膏类化妆品中壬基苯酚的测定。

Determination of nonylphenol in cosmetics.Liquid chromatography tandem mass spectrometry

SN/T 3716-2013 电子电气产品中壬基苯酚及壬基苯酚聚氧乙烯醚的测定 高效液相色谱法

本标准规定了电子电气产品中壬基苯酚(NP)及壬基苯酚聚氧乙烯醚(NPE-n,n=1~16)的高效液相色谱(HPLC)测定方法。本标准适用于电子电气产品中壬基苯酚及壬基苯酚聚氧乙烯醚的测定。

Determination of nonylphenol and nonylphenol polyethoxylate in electrical and electronic equipment.High performance liquid chromatography

ISO/TS 13907-2012 土质.气相色谱质谱法(GC-MS)测定基酚(NP)和单壬基苯酚和二乙基氧化物

Soil quality - Determination of nonylphenols (NP) and nonylphenol-mono- and diethoxylates - Method by gas chromatography with mass selective detection (GC-MS)

DIN CEN/TS 16182-2012 污泥, 经处理生物废弃物和土壤. 采用带质量选择性检测的气相色谱法(GC-MS)对壬基酚(NP), 壬基苯酚单乙氧基醇和壬基苯酚二乙氧基醇的测定; 德文版本CEN/TS 16182-2012

Sludge, treated biowaste and soil - Determination of nonylphenols (NP) and nonylphenol-mono- and diethoxylates using gas chromatography with mass selective detection (GC-MS); German version CEN/TS 16182:2012

ASTM D7065-2011 使用气相色谱质谱测定法测定环境水中壬基苯酚, 双酚A, 对特辛基苯酚, 壬基苯酚一乙氧醚和壬基苯酚二乙氧醚的标准试验方法

5. Significance and UseTop Bottom 5.1 Nonylphenol3, octylphenol, and bisphenol A have been shown to have toxic effects in aquatic organisms. The source of nonylphenol and octylphenol is prominently from the use of common commercial surfactants. The most widely used surfactant is NPEO which has an average ethoxylate chain of 9 mol of ethoxylate. The ethoxylate chain is readily biodegraded to form NP1EO and NP2EO, nonylphenol carboxylate (NPEC) and, under anaerobic conditions, nonylphenol. Nonylphenol will also biodegrade, but may be released into environmental waters directly at trace levels. This method has been investigated for use with surface water and waste treatment effluent samples and is applicable to these matrices. It has not been investigated for use with salt water or solid sample matrices. 5.2 The first reported synthesis of BPA was by the reaction of phenol with acetone by Zincke.4 BPA has become an important high volume industrial chemical used in the manufacture of polycarbonate plastics and epoxy resins. Polycarbonate plastic and resins are used in numerous products including electrical and electronic equipment, automobiles, sports and safety equipment, reusable food and drink containers, electrical laminates for printed circuit boards, composites, paints, adhesives, dental sealants, protective coatings and many other products.5 The environmental source of BPA is predominantly from the decomposition of polycarbonate plastics and resins. BPA is not classified as bio-accumulative by the U.S. Environmental Protection Agency and will biodegrade. BPA may be released into the environment waters directly at trace levels through landfill leachate and sewage treatment plant effluents. 1.1 This test method covers determination of nonylphenol (NP), nonylphenol ethoxylate (NP1EO), nonylphenol diethoxylate (NP2EO), octylphenol (OP), and bisphenol A (BPA) that are partitioned into organic solvent, separated using gas chromatography and detected with mass selective detection. These compounds or isomer mixtures are qualitatively and quantitatively determined by this method. This method adheres to selected ion monitoring mass spectrometry but full scan mass spectrometry has also been shown to work well under these conditions. Either analysis may be used. 1.2 The method detection limit (MDL) and reporting limit (RL) for NP, NP1EO, NP2EO, OP, and BPA are listed in Table 1.TABLE 1 MDL and Reporting Limits Analyte

Standard Test Method for Determination of Nonylphenol, Bisphenol A, p-tert -Octylphenol, Nonylphenol Monoethoxylate and Nonylphenol Diethoxylate in Environmental Waters by Gas Chromatography Mass Spectrometry

BS ISO 24293-2009 水质.壬基苯酚个别异构体的测定.采用固相萃取(SPE)和气相色谱/质谱联用法(GC/MS)

Water quality - Determination of individual isomers of nonylphenol - Method using solid phase extraction (SPE) and gas chromatography/mass spectrometry (GC/MS)

BS ISO 24293-2009 水质.壬基苯酚个别异构体的测定.采用固相萃取(SPE)和气相色谱/质谱联用法(GC/MS)

Water quality - Determination of individual isomers of nonylphenol - Method using solid phase extraction (SPE) and gas chromatography/mass spectrometry (GC/MS)

ASTM D7485-2009 用液相色谱/串联质谱法测定环境水域中的壬基酚,对叔辛基酚,对壬基苯酚一乙氧醚和对壬基苯酚二乙氧醚的标准试验方法

NP and OP have been shown to have toxic effects in aquatic organisms. The source of NP and OP is prominently from the use of common commercial surfactants. The most widely used surfactant is nonylphenol ethoxylate (NPEO) which has an average ethoxylate chain length of nine. The ethoxylate chain is readily biodegraded to form NP1EO, NP2EO, nonylphenol carboxylate (NPEC) and, under anaerobic conditions, NP. NP will also biodegrade, but may be released into environmental waters directly at trace levels. This method has been investigated and is applicable for environmental waters, including seawater.1.1 This test method covers the determination of nonylphenol (NP), nonylphenol ethoxylate (NP1EO), nonylphenol diethoxylate (NP2EO), and octylphenol (OP), extracted from water utilizing solid phase extraction (SPE), separated using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These compounds are qualitatively and quantitatively determined by this method. This method adheres to single reaction monitoring (SRM) mass spectrometry. 1.2 The method detection limit (MDL) and reporting limit (RL) for NP, NP1EO, NP2EO, and OP are listed in Table 1. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. TABLE 1 MDL and Reporting Limits AnalyteMDLA (ng/L)Reporting RangeB (ng/L) NP33100-2000 NP1EO9100-2000 NP2EO9100-2000 OP24100-2000 A MDL Determined Following The Code of Federal Regulations, 40 CFR Part 136, Appendix B. B Lowest Point of the Reporting Range is Calculated from the LV 1 Concentration Calibration Standard in Table 4.

Standard Test Method for Determination of Nonylphenol, p-tert-Octylphenol, Nonylphenol Monoethoxylate and Nonylphenol Diethoxylate in Environmental Waters by Liquid Chromatography/Tandem Mass Spectrometry

JIS K0450-60-10-2007 工业水和废水中游离的4-壬基苯酚异构体的测试方法

この規格は，工業用水及び工場排水中の4ーノニルフエノール(CAS No.25154-52-3)の異性体のうち，表1の異性体を，ガスクロマトグラ7質量分析法を用いて定量する試験方法について規定する。

Testing method for individual 4-nonylphenol isomers in industrial water and wastewater

JIS K 0450-60-10-2007 工业水和废水中游离的4-壬基苯酚异构体的测试方法

Testing method for individual 4-nonylphenol isomers in industrial water and wastewater