呋线威检测

(EU) No 2019-0552 就嘧菌酯、氟吡草酮、矮壮素、嘧菌环胺、苯醚甲环唑、丁苯吗啉、唑螨酯、氟吡菌酰胺、三乙膦酸铝、稻瘟灵、吡唑萘菌胺、杀线威、丙硫菌唑、乙基多杀菌素、肟菌酯和2,4-二氧-1-(5-甲基嘧啶)-3-[3-三氟甲基苯基-2H-吡啶并[1,2-α]]吡啶内盐在部分农产品内部或表面的最大残留限量，修订欧洲议会和理事会条例(EC) No 396/2005 的附件II、III

ASTM D7600-2016 采用液相色谱法/串联质谱法测定涕灭威, 呋喃丹, 杀线威和灭多威的标准试验方法

5.1x00a0;The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water.4 5.2x00a0;This test method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl, and methomyl. 1.1x00a0;This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this test method. This test method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2x00a0;This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL). 1.3x00a0;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4x00a0;The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.4.1x00a0;The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.4.2x00a0;The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.5x00a0;This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Determination of Aldicarb, Carbofuran, Oxamyl and Methomyl by Liquid Chromatography/Tandem Mass Spectrometry

ASTM D7645-2016 采用液相色谱法/串联质谱法 (LC/MS/MS) 测定水中涕灭威, 涕灭威砜, 涕灭威亚砜, 呋喃丹, 灭多威, 杀线威和久效威的标准试验方法

5.1x00a0;This test method has been developed by U.S. EPA Region 5 Chicago Regional Laboratory (CRL). 5.2x00a0;The N-methyl carbamate (NMC) pesticides: aldicarb, carbofuran, methomyl, oxamyl, and thiofanox have been identified by EPA as working through a common mechanism. These affect the nervous system by reducing the ability of enzymes. Enzyme inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water, and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water. Aldicarb sulfone and aldicarb sulfoxide are breakdown products of aldicarb and should also be monitored due to their toxicological effects.4 5.3x00a0;This test method has been investigated for use with reagent, surface, and drinking water for the selected carbamates: aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl, and thiofanox. 1.1x00a0;This procedure covers the determination of aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl, and thiofanox (referred to collectively as carbamates in this test method) in water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this test method. This test method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2x00a0;The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.2.1x00a0;The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions, and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.2.2x00a0;The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.3x00a0;Unitsx2014;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4x00a0;This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior ......

Standard Test Method for Determination of Aldicarb, Aldicarb Sulfone, Aldicarb Sulfoxide, Carbofuran, Methomyl, Oxamyl, and Thiofanox in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)

SN/T 0697-2014 出口肉及肉制品中杀线威残留量的测定

本标准规定了出口肉及肉制品中杀线威残留量测定的液相色谱-质谱/质谱和高效液相色谱检测方法。 本标准适用于出口猪肉、牛肉、羊肉、鸡肉、香肠中杀线威残留量的测定。

Determination of oxamyl residue in meat and meat product for export

SN/T 1017.7-2014 出口粮谷中涕灭威、甲萘威、杀线威、恶虫威、抗蚜威残留量的测定

SN/T 1017的本部分规定了出n粮谷中涕灭威、甲萘威、杀线威、恶虫威、抗蚜威残留量的液相色谱-质谱/质谱和液相色谱的测定方法。本部分适用于出口大米、玉米、小麦和大豆中涕灭威、甲萘威、杀线威、恶虫威、抗蚜威五种氨基甲酸酯类农药残留量的测定。

Determination of aldicarb,carbryl,oxamyl,bendiocarb and pirimicarb residues in cereals for export

ASTM D7645-2014 使用液相色谱法/串联质谱法测定水中涕灭威, 涕灭威砜, 涕灭威亚砜, 克百威, 灭多威, 杀线威和久效威的标准试验方法

5.1x00a0;This test method has been developed by U.S. EPA Region 5 Chicago Regional Laboratory (CRL). 5.2x00a0;The N-methyl carbamate (NMC) pesticides: aldicarb, carbofuran, methomyl, oxamyl, and thiofanox have been identified by EPA as working through a common mechanism. These affect the nervous system by reducing the ability of enzymes. Enzyme inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water, and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water. Aldicarb sulfone and aldicarb sulfoxide are breakdown products of aldicarb and should also be monitored due to their toxicological effects.4 5.3x00a0;This test method has been investigated for use with reagent, surface, and drinking water for the selected carbamates: aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl, and thiofanox. 1.1x00a0;This procedure covers the determination of aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl, and thiofanox (referred to collectively as carbamates in this test method) in water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This test method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2x00a0;The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.2.1x00a0;The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions, and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.2.2x00a0;The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.3x00a0;Unitsx2014;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4x00a0;This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Determination of Aldicarb, Aldicarb Sulfone, Aldicarb Sulfoxide, Carbofuran, Methomyl, Oxamyl, and Thiofanox in Water by Liquid Chromatography/Tandem Mass Spectrometry 40;LC/MS/MS41;

SN/T 0134-2010 进出口食品中杀线威等12种氨基甲酸酯类农药残留量的检测方法.液相色谱-质谱/质谱法

本标准规定了食品中纱线威、灭多威、抗蚜威、涕灭威、速灭威、克百威、甲萘威、乙硫甲威、异丙威、乙霉威和仲丁威等12中氨基甲酸酯类农药残留量的液相色谱-质谱/质谱检测方法。 本标准适用于玉米、糙米、大麦、白菜、大葱、小麦、大豆、花生、苹果、柑橘、牛肝、鸡肾和蜂蜜中杀线威、灭多威、抗蚜威、涕灭威、速灭威、克百威、甲萘威、乙硫甲威、异丙威、乙霉威和仲丁威残留量的检测和确证。

Determination for pesticide residues of 12 kinds of carbamates including oxamyl in foods for import and export.LC-MS/MS method

ASTM D7645-2010e1 用液相色谱法/串联质谱检测法(LC/MS/MS)测定水中涕灭威,涕灭威砜,涕灭威亚砜,克百威,灭多威,杀线威和久效威的标准试验方法

This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL). The N-methyl carbamate (NMC) pesticides: aldicarb, carbofuran, methomyl, oxamyl, and thiofanox have been identified by EPA as working through a common mechanism. These affect the nervous system by reducing the ability of enzymes. Enzyme inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water, and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water. Aldicarb sulfone and aldicarb sulfoxide are breakdown products of aldicarb and should also be monitored due to their toxicological effects. This method has been investigated for use with reagent, surface, and drinking water for the selected carbamates: aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl and thiofanox.1.1 This test method covers the determination of aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl, and thiofanox (referred to collectively as carbamates in this test method) in water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2 The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.2.1 The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions, and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.2.2 The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.3 Units8212;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. TABLE 1 Detection Verification Level and Reporting Range AnalyteDVL (ng/L)Reporting Range (x03BC;g/L) Aldicarb2501-100 Aldicarb Sulfone2501-100 Aldicarb Sulfoxide2501-100 Carbofuran2501-100 Methomyl2501-100

Standard Test Method for Determination of Aldicarb, Aldicarb Sulfone, Aldicarb Sulfoxide, Carbofuran, Methomyl, Oxamyl and Thiofanox in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)

ASTM D7645-2010 液相色谱/串联质谱法测定水中涕灭威，涕灭威砜，涕灭威亚砜，克百威，灭多威，杀线威和久效威的标准试验方法

This test method has been developed in support of the National Homeland Security Research Center, US EPA by Region 5 Chicago Regional Laboratory (CRL). The N-methyl carbamate (NMC) pesticides: aldicarb, carbofuran, methomyl, oxamyl, and thiofanox have been identified by EPA as working through a common mechanism. These affect the nervous system by reducing the ability of enzymes. Enzyme inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water, and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water. Aldicarb sulfone and aldicarb sulfoxide are breakdown products of aldicarb and should also be monitored due to their toxicological effects. This method has been investigated for use with reagent, surface, and drinking water for the selected carbamates: aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl and thiofanox.1.1 This test method covers the determination of aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl, and thiofanox (referred to collectively as carbamates in this test method) in water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2 The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.2.1 The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions, and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.2.2 The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.3 Units8212;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Determination of Aldicarb, Aldicarb Sulfone, Aldicarb Sulfoxide, Carbofuran, Methomyl, Oxamyl and Thiofanox in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)

ASTM D7600-2009 液相色谱串联质谱法测定涕灭威、克百威、杀线威及灭多威的标准试验方法

The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water. This method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl and methomyl.1.1 This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2 This test method has been developed in support of the National Homeland Security Research Center, US EPA by Region 5 Chicago Regional Laboratory. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.4.1 The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.4.2 The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Determination of Aldicarb, Carbofuran, Oxamyl and Methomyl by Liquid Chromatography/Tandem Mass Spectrometry

ASTM D7600-2009e1 液相色谱串联质谱法测定涕灭威,克百威,杀线威及灭多威的标准试验方法

The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water. This method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl and methomyl.1.1 This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2 This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL). 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.4.1 The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.4.2 The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. TABLE 1 Detection Verification Level and Reporting Range AnalyteDVL (x03BC;g/L)Reporting Range (x03BC;g/L) Aldicarb1001x2013;100 Carbofuran1001x2013;100 Oxamyl1001x2013;100 Methomyl1001x2013;100 TABLE 2 Concentrations of Calibration Standards (PPB) Analyte/Surrogate LV 1LV 2LV 3LV 4

Standard Test Method for Determination of Aldicarb, Carbofuran, Oxamyl and Methomyl by Liquid Chromatography/Tandem Mass Spectrometry

ASTM D7600-2009e2 使用液相色谱法/串联质谱法测定涕灭威, 克百威, 杀线威及灭多威的标准试验方法

5.1x00a0;The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water.4 5.2x00a0;This method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl and methomyl. 1.1x00a0;This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2x00a0;This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL). 1.3x00a0;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4x00a0;The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. TABLE 1 Detection Verification Level and Reporting Range Analyte DVL (ng/L)x2020; Reporting Range (x03bc;g/L)

Standard Test Method for Determination of Aldicarb, Carbofuran, Oxamyl and Methomyl by Liquid Chromatography/Tandem Mass Spectrometry

ASTM D7600-2009e3 使用液相色谱法/串联质谱法测定涕灭威, 克百威, 杀线威及灭多威的标准试验方法

5.1x00a0;The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water.4 5.2x00a0;This method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl and methomyl. 1.1x00a0;This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2x00a0;This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL). 1.3x00a0;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4x00a0;The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.4.1x00a0;The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.4.2x00a0;The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.5x00a0;This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Determination of Aldicarb, Carbofuran, Oxamyl and Methomyl by Liquid Chromatography/Tandem Mass Spectrometry

SN/T 1017.7-2002 出口粮谷中涕灭威、西维因、杀线威、恶虫威、抗蚜威残留量的检验方法

Method for the determination of aldicarb,carbryl.oxamyl,bendiocarb and pirimicarb residues in cereals for export

SN 0697-1997 出口肉及肉制品中杀线威残留量检验方法.液相色谱法

Method for the determination of oxamyl residues in meats and meat products for export.Liquid chromatographic method

MSZ 21470/32-1982 土壤的环保测试．杀线威的含量测定

ANSI K62.126-1972 杀线威(oxamyl)－(杀虫剂和杀线虫剂)通用名称

Provides the accepted common name for the chemical compound given. Includes the use of the common name and the physical and chemical properties of the chemical compound.

Common Name for the Pest Control Chemical Methyl N',N'-Dimethyl-N- ((Methylcarbamoyl) Oxy)- 1-Thiooxamimidate "Oxamyl"

JAP-139 涕灭威、乙硫甲威、杀线威、甲萘威、抗芽威、仲丁威和恶虫威检测方法