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灭多威检测

发布时间:2024-05-27 17:49:26 - 更新时间:2024年06月29日 15:22

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军工检测 其他检测

GB 24752-2009 灭多威原药

本标准规定了灭多威原药的要求、试验方法以及标志、标签、包装、贮运。 本标准适用于由灭多威及其生产中产生的杂质组成的灭多威原药。

Methomyl technical

GB 23557-2009 灭多威乳油

本标准规定了20%灭多威乳油的要求、试验方法以及标志、标签、包装、贮运。 本标准适用于由灭多威原药与乳化剂溶解在适宜的溶剂中配制成的20%灭多威乳油。

Methomyl emulsifiable concentrates

GA/T 1619-2019 法庭科学 生物检材中灭多威和灭多威肟检验 气相色谱-质谱和液相色谱-质谱法

KJ 201710 蔬菜中敌百虫、丙溴磷、灭多威、克百威、敌敌畏残留的快速检测

本方法规定了蔬菜中敌百虫、丙溴磷、灭多威、克百威、敌敌畏残留的快速检测方法。本方法适用于油菜、菠菜、芹菜、韭菜等蔬菜中敌百虫、丙溴磷、灭多威、克百威、敌敌畏残留的快速测定。

HJ 851-2017 水质 灭多威和灭多威肟的测定 液相色谱法

HJ 851-2017 水质灭多威和灭多威肟的测定 液相色谱法

本标准规定了测定水中灭多威和灭多威肟的液相色谱法。 本标准适用于地表水、地下水、生活污水和工业废水中灭多威和灭多威肟的测定。 当进样量为 50 μl时,灭多威和灭多威肟的方法检出限均为 1μg/L,测定下限均为 4μg/L。

Water quality - Determination of methomyl and methomyl-oxime - High performance liquid chromatography

(EU) No 2016-1822 就苯草醚、溴氰菊酯、氟啶胺、灭多威、磺草酮和硫双威在部分产品中的最大残留限量修订欧洲议会和理事会条例(EC) No 396/2005附录II和III

ASTM D7645-2016 采用液相色谱法/串联质谱法 (LC/MS/MS) 测定水中涕灭威, 涕灭威砜, 涕灭威亚砜, 呋喃丹, 灭多威, 杀线威和久效威的标准试验方法

5.1x00a0;This test method has been developed by U.S. EPA Region 5 Chicago Regional Laboratory (CRL). 5.2x00a0;The N-methyl carbamate (NMC) pesticides: aldicarb, carbofuran, methomyl, oxamyl, and thiofanox have been identified by EPA as working through a common mechanism. These affect the nervous system by reducing the ability of enzymes. Enzyme inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water, and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water. Aldicarb sulfone and aldicarb sulfoxide are breakdown products of aldicarb and should also be monitored due to their toxicological effects.4 5.3x00a0;This test method has been investigated for use with reagent, surface, and drinking water for the selected carbamates: aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl, and thiofanox. 1.1x00a0;This procedure covers the determination of aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl, and thiofanox (referred to collectively as carbamates in this test method) in water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this test method. This test method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2x00a0;The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.2.1x00a0;The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions, and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.2.2x00a0;The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.3x00a0;Unitsx2014;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4x00a0;This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior ......

Standard Test Method for Determination of Aldicarb, Aldicarb Sulfone, Aldicarb Sulfoxide, Carbofuran, Methomyl, Oxamyl, and Thiofanox in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)

ASTM D7600-2016 采用液相色谱法/串联质谱法测定涕灭威, 呋喃丹, 杀线威和灭多威的标准试验方法

5.1x00a0;The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water.4 5.2x00a0;This test method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl, and methomyl. 1.1x00a0;This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this test method. This test method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2x00a0;This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL). 1.3x00a0;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4x00a0;The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.4.1x00a0;The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.4.2x00a0;The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.5x00a0;This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Determination of Aldicarb, Carbofuran, Oxamyl and Methomyl by Liquid Chromatography/Tandem Mass Spectrometry

ASTM D7645-14 用液相色谱/串联质谱法测定水中涕灭威、涕灭威砜、涕灭威亚砜、呋喃丹、灭多威、恶戊醇和噻凡诺的标准试验方法(;LC/MS/MS)

Standard Test Method for Determination of Aldicarb, Aldicarb Sulfone, Aldicarb Sulfoxide, Carbofuran, Methomyl, Oxamyl, and Thiofanox in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC

ASTM D7645-2014 使用液相色谱法/串联质谱法测定水中涕灭威, 涕灭威砜, 涕灭威亚砜, 克百威, 灭多威, 杀线威和久效威的标准试验方法

5.1x00a0;This test method has been developed by U.S. EPA Region 5 Chicago Regional Laboratory (CRL). 5.2x00a0;The N-methyl carbamate (NMC) pesticides: aldicarb, carbofuran, methomyl, oxamyl, and thiofanox have been identified by EPA as working through a common mechanism. These affect the nervous system by reducing the ability of enzymes. Enzyme inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water, and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water. Aldicarb sulfone and aldicarb sulfoxide are breakdown products of aldicarb and should also be monitored due to their toxicological effects.4 5.3x00a0;This test method has been investigated for use with reagent, surface, and drinking water for the selected carbamates: aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl, and thiofanox. 1.1x00a0;This procedure covers the determination of aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl, and thiofanox (referred to collectively as carbamates in this test method) in water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This test method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2x00a0;The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.2.1x00a0;The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions, and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.2.2x00a0;The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.3x00a0;Unitsx2014;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4x00a0;This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Determination of Aldicarb, Aldicarb Sulfone, Aldicarb Sulfoxide, Carbofuran, Methomyl, Oxamyl, and Thiofanox in Water by Liquid Chromatography/Tandem Mass Spectrometry 40;LC/MS/MS41;

ASTM D7645-2010e1 用液相色谱法/串联质谱检测法(LC/MS/MS)测定水中涕灭威,涕灭威砜,涕灭威亚砜,克百威,灭多威,杀线威和久效威的标准试验方法

This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL). The N-methyl carbamate (NMC) pesticides: aldicarb, carbofuran, methomyl, oxamyl, and thiofanox have been identified by EPA as working through a common mechanism. These affect the nervous system by reducing the ability of enzymes. Enzyme inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water, and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water. Aldicarb sulfone and aldicarb sulfoxide are breakdown products of aldicarb and should also be monitored due to their toxicological effects. This method has been investigated for use with reagent, surface, and drinking water for the selected carbamates: aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl and thiofanox.1.1 This test method covers the determination of aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl, and thiofanox (referred to collectively as carbamates in this test method) in water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2 The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.2.1 The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions, and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.2.2 The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.3 Units8212;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. TABLE 1 Detection Verification Level and Reporting Range AnalyteDVL (ng/L)Reporting Range (x03BC;g/L) Aldicarb2501-100 Aldicarb Sulfone2501-100 Aldicarb Sulfoxide2501-100 Carbofuran2501-100 Methomyl2501-100

Standard Test Method for Determination of Aldicarb, Aldicarb Sulfone, Aldicarb Sulfoxide, Carbofuran, Methomyl, Oxamyl and Thiofanox in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)

ASTM D7645-2010 液相色谱/串联质谱法测定水中涕灭威,涕灭威砜,涕灭威亚砜,克百威,灭多威,杀线威和久效威的标准试验方法

This test method has been developed in support of the National Homeland Security Research Center, US EPA by Region 5 Chicago Regional Laboratory (CRL). The N-methyl carbamate (NMC) pesticides: aldicarb, carbofuran, methomyl, oxamyl, and thiofanox have been identified by EPA as working through a common mechanism. These affect the nervous system by reducing the ability of enzymes. Enzyme inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water, and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water. Aldicarb sulfone and aldicarb sulfoxide are breakdown products of aldicarb and should also be monitored due to their toxicological effects. This method has been investigated for use with reagent, surface, and drinking water for the selected carbamates: aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl and thiofanox.1.1 This test method covers the determination of aldicarb, aldicarb sulfone, aldicarb sulfoxide, carbofuran, methomyl, oxamyl, and thiofanox (referred to collectively as carbamates in this test method) in water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2 The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.2.1 The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions, and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.2.2 The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.3 Units8212;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Determination of Aldicarb, Aldicarb Sulfone, Aldicarb Sulfoxide, Carbofuran, Methomyl, Oxamyl and Thiofanox in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)

ASTM D7600-2009e2 使用液相色谱法/串联质谱法测定涕灭威, 克百威, 杀线威及灭多威的标准试验方法

5.1x00a0;The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water.4 5.2x00a0;This method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl and methomyl. 1.1x00a0;This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2x00a0;This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL). 1.3x00a0;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4x00a0;The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. TABLE 1 Detection Verification Level and Reporting Range Analyte DVL (ng/L)x2020; Reporting Range (x03bc;g/L)

Standard Test Method for Determination of Aldicarb, Carbofuran, Oxamyl and Methomyl by Liquid Chromatography/Tandem Mass Spectrometry

ASTM D7600-2009e3 使用液相色谱法/串联质谱法测定涕灭威, 克百威, 杀线威及灭多威的标准试验方法

5.1x00a0;The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water.4 5.2x00a0;This method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl and methomyl. 1.1x00a0;This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2x00a0;This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL). 1.3x00a0;The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4x00a0;The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.4.1x00a0;The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.4.2x00a0;The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.5x00a0;This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Determination of Aldicarb, Carbofuran, Oxamyl and Methomyl by Liquid Chromatography/Tandem Mass Spectrometry

ASTM D7600-2009e1 液相色谱串联质谱法测定涕灭威,克百威,杀线威及灭多威的标准试验方法

The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water. This method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl and methomyl.1.1 This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2 This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL). 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.4.1 The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.4.2 The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. TABLE 1 Detection Verification Level and Reporting Range AnalyteDVL (x03BC;g/L)Reporting Range (x03BC;g/L) Aldicarb1001x2013;100 Carbofuran1001x2013;100 Oxamyl1001x2013;100 Methomyl1001x2013;100 TABLE 2 Concentrations of Calibration Standards (PPB) Analyte/Surrogate LV 1LV 2LV 3LV 4

Standard Test Method for Determination of Aldicarb, Carbofuran, Oxamyl and Methomyl by Liquid Chromatography/Tandem Mass Spectrometry

ASTM D7600-2009 液相色谱串联质谱法测定涕灭威、克百威、杀线威及灭多威的标准试验方法

The N-methyl carbamate (NMC) pesticides: aldicarb, carbaryl, carbofuran, formetanate hydrochloride, methiocarb, methomyl, oxamyl, pirimicarb, propoxur, and thiodicarb have been identified by EPA as working through a common mechanism. They affect the nervous system by reducing the ability of the enzyme cholinesterase. Cholinesterase inhibition was the primary toxicological effect of regulatory concern to EPA in assessing the NMCx2019;s food, drinking water and residential risks. In most of the country, NMC residues in drinking water sources are at levels that are not likely to contribute substantially to the multi-pathway cumulative exposure. Shallow private wells extending through highly permeable soils into shallow, acidic ground water represent what the EPA believes to be the most vulnerable drinking water. This method has been investigated for use with reagent and surface water for the selected carbamates: aldicarb, carbofuran, oxamyl and methomyl.1.1 This procedure covers the determination of aldicarb, carbofuran, oxamyl and methomyl (referred to collectively as carbamates in this test method) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2 This test method has been developed in support of the National Homeland Security Research Center, US EPA by Region 5 Chicago Regional Laboratory. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 The Detection Verification Level (DVL) and Reporting Range for the carbamates are listed in Table 1. 1.4.1 The DVL is required to be at a concentration at least 3 times below the Reporting Limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratios of the primary single reaction monitoring (SRM) transitions and Fig. 2 displays the confirmatory SRM transitions at the DVLs for the carbamates. 1.4.2 The reporting limit is the concentration of the Level 1 calibration standard as shown in Table 2 for the carbamates. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Determination of Aldicarb, Carbofuran, Oxamyl and Methomyl by Liquid Chromatography/Tandem Mass Spectrometry

YC/T 219-2007 烟草及烟草制品 灭多威农药残留量的测定 气相色谱法

本标准规定了烟草中灭多威农药残留量的气相色谱测定方法。 本标准适用于烟草和烟草制品。

Tobacco and tobacco products Determination of methomyl residues Gas chromatographic method

DB13/ 359-1998 硫双灭多威原药

本标准由河北省石油化工厅提出。本标准规定了硫双灭多威原药的技术要求、试验方法、检验规则以及标志、包装、运输和贮存。 本标准适用于以灭多威和二氮化硫为原料生产的硫双灭多威原药。 硫双灭多威的其它名称、结构式和基本物化参数如下: ISO通用.名称:thiodicarb 化学名称:3,7,9,13-四甲基-5,11-二氧-2.8,14-三硫-4, 7,9,12-四氮十五烷-3,12-乙烯-6,11-二酮. 实验式:C10H18N4O4S8 相对分子质量:354.46(按1993年国际相对原子质量计) 生物活性:杀虫。 熔点:173℃一174℃ 蒸汽压(251C):5.1mPa, 溶解度(g/1,200C):水0.035;丙酮8;二甲苯3, 稳定性:60℃稳定;其水悬液因日光而分解,PH6稳定, PH9迅速水解,PH3缓慢水解;DT50约为9d;遇酸、碱,金属 盐、黄铜和铁锈易分解。

SN 0582-1996 出口粮谷及油籽中灭多威残留量检验方法

Method for the determination of methomyl residues in cereals and oil seeds for export

HG 2612-1994 灭多威乳油

本标准规定了灭多威乳油的技术要求、试验方法、检验规则及标志、包装、运输和贮存要求。 本标准适用于由灭多威原药与乳化剂溶解在适宜的溶剂中配制成的乳油。

HG 2611-1994 灭多威原药

本标准规定了灭多威原药的技术要求、试验方法、检验规则及标志、包装,运输和贮存要求。 本标准适用于灭多威原药及生产中产生的杂质组成的灭多威原药,应外来杂质和添加的改性剂。

ANSI K62.220-1979 硫双灭多威(thiodicarb)-(杀虫剂)通用名称

Provides the accepted common name for the chemical compound given. Includes the use of the common name and the physical and chemical properties of the chemical compound.

Common Name for the Pest Control Chemical Dimethyl N,N'-(thio-bis(methylimino) carbonyloxy )bis (ethanimidothioate) "Thiodicarb"

ANSI K62.70-1967 灭多威(methomyl)-(杀虫剂)通用名称

Provides the accepted common name for the chemical compound given. Includes the use of the common name and the physical and chemical properties of the chemical compound.

Common Name for the Pest Control Chemical S-Methyl N- ((methylcarbamoyl)oxy) thioacetimidate Methomyl

DB31/ 133-1994 20%灭多威乳油

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